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Roasting zinc sulphide ores..
Chloridizing roasting.
Oxide roasting......
Sulphate roasting.
Roasting of a low-iron ore from Daly-Judge mine..
Description of ore and of method used....
Discussion of results of tests.
Leaching the calcine........
Roasting of a high-iron ore from Honorine mine.
Effects of temperature and time of roasting.
Effects of fineness of grinding......
Experiments to determine the effects of lead..
Leaching the calcined ore.....
General method used in tests...
Tests of ore from Daly-Judge mine.....
Tests of ore from Bullion Coalition mine...
Effects of roasting with sodium chloride..
Treatment of low-lead mill products..
Tests of marmatite ore from Wasa mine.
Tests of partly oxidized ores....
Ore from Lower Mammoth mine.
Marmatite ore from Wasa mine...
Magnetic roasting...
Hydrometallurgy of zinc sulphide ores.
Sulphate processes.......
Sulphite processes.
Difficulties of applying process..
Precipitation of zinc sulphate solutions with calcium chloride.
Precipitation of zinc chloride with lime.
Tests with pure zinc chloride...................
Experiment with oxidized zinc ore.
Removal of manganese.....
Use of chloride of lime in moderate amounts....
Use of larger amounts of chloride of lime..
Use of zinc chloride solution...
Tests with chlorine water..
Tests with chlorine gas...
Bisulphite solutions...
Summary...
Page.
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Publications available for free distribution....
Publications that may be obtained only through the Superintendent of
138
Documents....
Index.......
139
141
TABLES.
TABLE 1. Production of spelter in the United States in 1914...
2. Recovery of zinc by various concentration processes.
12
3. Analyses of oxidized and semioxidized zinc ores..
21
4. Analyses of complex zinc-sulphide ores and concentrates.
2822
18
5. Names of shippers from Park City district during 1915, with ton-
nage and products shipped.....
6. Mill tests at the Daly-Judge mill...
7. Results of magnetic separation of Utah-Apex zinc-iron middling..
8. Results of magnetic separation of ore from Consolidated Nevada-
Utah mine..
9. Results of magnetic separation of ore from Greenwood lease..........
10. Results of magnetic concentration of zinc middling from the Broad-
water mill....
48
49
11. Results of magnetic separation of ore from Carlyle mine, roasting
without tabling.
50
12. Results of magnetic separation of ore from Carlyle mine, with
tabling...
TABLE 13. Results of magnetic separation of ore from C. O. D. mine near
Chloride, Ariz...........
14. Results of concentration tests of ore from Middle Golconda mine...
15. Results of analyses of zinc-lead sulphide ores.
16. Results of leaching Daly-Judge calcines........
17. Results of leaching calcines from the roasting of Bullion Coalition
No. 5 ore..
66
18. Results of leaching calcines from chloridizing roast of Bullion
Coalition No. 5 ore....
19. Results of analyses of four zinc products low in lead.........
20. Results of screen analyses of zinc ores and concentrates low in lead.. 69
21. Leaching zinc blende from Joplin, Mo., after roasting................
22. Results of leading zinc-blende concentrate and zinc-iron middling
from Midvale, Utah, after roasting.
67
69
70
23. Results of leaching ore from Wasa mine after roasting at 750° C. for
4 hours.....
24. Results of screen analysis of partly oxidized ores from Lower Mam-
moth mine after roasting....
25. Results of roasting and leaching partly oxidized zinc ore, Lower
Mammoth No. 1..
26. Roasting and leaching partly oxidized zinc ore, Lower Mammoth
No. 2...
71
27. Results of roasting and sulphuric acid leaching, ore from Wasa mine..
28. Precipitation of sulphates from zinc sulphate solutions with calcium
chloride...
29. Precipitation of zinc chloride solutions with lime.......
30. Results of treating zinc-sulphate leaching solutions with lime com-
pounds.......
31. Results of treating zinc sulphate solutions with lime compounds for
removal of manganese.......
32. Results of treating zinc sulphate solutions with excess CaOCl2 to
remove manganese.......
33. Results of treating zinc hydroxide precipitate with zinc chloride
solution to remove lime.
34. Results of treating zinc sulphate solutions with chlorine to oxidize
manganese..
35. Results of cyclic leaching and precipitation tests..
99
36. Results of calcining oxidized zinc ores..
106
37. Results of igneous concentration of oxidized zinc ore in a small
blast furnace..........
109
38. Results of igneous concentration of low-grade sulphide ores of lead
and zinc in a small blast furnace....
110
39. Costs and profits of a 25-ton zinc oxide plant.....
40. Costs and profits of a 50-ton zinc oxide plant...
116
118
41. Compositions of oxidized zinc ores used in leaching tests with
sulphuric acid...................
125
42. Results of trial leaches on 1-gram samples of oxidized ores...
43. Results of leaching oxidized zinc ores with sulphuric acid, showing
zinc recovery and acid efficiency...
126
44. Results of analyses of neutral solution of zinc sulphate and
impurities....
127
45. Results of sulphurous acid leaching of oxidized zinc ores..
131
46. Results of leaching oxidized zinc ore with caustic soda solution....
133
ILLUSTRATIONS.
FIGURE 1. Present source of zinc and also ores not utilized.....
2. Curves showing effect of temperature on speed of roasting, Daly-
Judge No. 1 sample....
14
3. Curves showing effects of leaching with different solvents, Daly-
Judge No. 1 sample.....................
58
4. Curves showing effect of temperature on speed of roasting, Bullion
Coalition No. 5 sample.......
5. Curves showing effects of size of ore on speed of roasting, Bullion
6. Curves showing effects of temperature on solubility of zinc and
lead in slime from Horn Silver dump, Frisco, Utah...
7. Curves showing effects of roasting on solubility of zinc and lead
in various ores.
8. Curves showing effects of roasting on solubility of zinc and iron in
semioxidized zinc ore from Lower Mammoth mine.......
75
9. Curves showing effect of strength of sulphurous acid on velocity of
solution of zinc oxide...............
10. Labratory blast furnace used for zinc-oxide experiments.....
11. Curves showing net smelter prices for oxidized zinc ores at Salt
Lake City.......
12 Curves showing change in value of zinc oxide concentrate with vary-
ing zinc content....
113
114
13. Plan and sections of 25-ton zinc-oxide plant...............
14. Curves showing cost per ton of ore for a 25-ton igneous concentra-
tion plant and returns as calculated from "ore" contract.........
15. Curves showing cost per ton of ore for a 25-ton igneous concentra-
tion plant and returns as calculated from "zinc oxide" contract.
16. Curves showing cost per ton of ore for a 50-ton igneous concentra-
tion plant and returns based on "ore" contract..
117
17. Curves showing cost per ton of ore for a 50-ton igneous concentra-
tion plant and returns as calculated from “zinc oxide" contract. 119
18. Curves showing efficiency of weak acids in four successive leaches. 122
19. Curves showing recovery of zinc in four successive leaches with
weak acids.....
122
20. Curves showing relation of zinc recovery to molecular weights of
acids used................
21. Curves showing effect of different concentrations of sulphuric acid.
22. Curves showing effects of different concentrations of hydrochloric
acid.......
123
23. Curves for computing acid efficiency when weights of acids con-
sumed and zinc recovered are known...
124